Vysoká škola
chemicko-technologická v Praze:
Jméno a
příjmení: Vladimír Kocourek |
Tituly: doc. Ing. CSc. |
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Přednášky v předmětech:
Legislativa a management jakosti
Kvalita v laboratorní kontrole potravin
Absolvovaná VŠ: VŠCHT Praha |
Rok: 1975 |
Praxe od absolvování VŠ: |
Od: |
Do: |
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VÚAB Roztoky u Prahy |
1975 |
1976 |
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VÚ potravinářského průmyslu Praha |
1981 |
1989 |
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Česká
zemědělská a potravinářská inspekce, Praha |
1989 |
1992 |
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Český ekologický ústav Praha |
1992 |
1993 |
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VŠCHT Praha |
1994 |
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Nejdůležitější publikace a další tvůrčí činnost za posledních pět let:
2.
Fast
temperature programming in routine analysis of multiple pesticide residues in
food matrices. J.CHROMATOG A 907 (2001) 235-245 (Podíl: 25 %)
3.
Focused
microwave (FMW) extraction of polycyclic aromatic hydrocarbons (PAHs) from plant
bioindicators. Polycyclic aromatic compounds 19 (2000) 217-226 (Podíl: 25 %)
4.
Sample
handling in analysis of pesticide residues in foodstuffs CHEMICKE LISTY 92 (10)
(1998) 777-783 (Podíl: 33 %)
5.
Stability
of pesticides in plant extracts used as calibrants in the gas chromatographic
analysis of residues. J. CHROMATOG A 800 (1998) 297-304 (Podíl: 35 %)
6.
Occurrence
of PAHs in environmental compartments - Alternative ways of monitoring.
CRITICAL REVIEWS IN ANALYTICAL CHEMISTRY 29 (1999) 123-124 1999 (Podíl: 25 %)
7.
Quality
assurance in planar PCBs analysis - validation of the method and results from
freshwater fish analysis. Organohalogen compounds 45 (2000) 134 - 137 (Podíl:
30 %)
8.
Matrix-
induced effects: critical point in GC analysis of pesticide residues. J.
CHROMATOG A 800 (1998) 283-295 (Podíl: 25 %)
Anotace nejvýznamnějších
publikací, projektů, děl a další tvůrčí čin.:
·
Analytical
method for the determination of ultra-trace levels of nitro-PAHs in various
biotic matrices has been developed. Soxhlet extraction and/or solvent
extraction enhanced by sonication were used for isolation of target analytes;
GPC followed by SPE were employed for purification of crude extracts. GC-MS/NCI
technique was utilised for identification/quantitation of target analytes.
Performance characteristics of implemented method were obtained through
thorough in-house validation procedure. The main sources of uncertainties were
critically evaluated, possible strategies of their elimination/minimisation
were considered and consequently employed. Examination of real-life samples of
various foodstuffs (complete human diet, mate tea, pumpkin seed oil, parsley,
sausages) was performed in this study.
·
Flash
gas chromatographic (GC) analysis of 15 organophosphorus pesticides commonly
occurring in food crops was performed using the Thermedics Detection EZ Flash
upgrade kit installed in the oven of a HP 5890 Series II Plus gas
chromatograph. The temperature program and splitless time period were the main
parameters to be optimized. In the first set of experiments wheat
matrix-matched standards were analyzed both by: (i) the flash GC technique
(resistive heating of a 5 m capillary column), and (ii) the conventional GC
technique (moderate oven temperature programming of a 30 m capillary column).
File translated from TEX by TTH, version 3.20.
On 01 Apr 2003, 13:34.